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Open AccessDOI: 10.1007/s12613-024-1234-5Original Research

A Novel Approach for Enhancing the Mechanical Properties of NiTi Shape Memory Alloys via Severe Plastic Deformation

🇨🇳 Original Chinese Title: A Novel Approach for Enhancing the Mechanical Properties of NiTi Shape Memory Alloys via Severe Plastic Deformation

Y. Zhang¹,L. Wang¹,H. Chen¹,X. Liu¹

School of Materials Science and Engineering, University of Science and Technology Beijing

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A Novel Approach for Enhancing the Mechanical Properties of NiTi Shape Memory Alloys via Severe Plastic Deformation
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Published In
Chinese Journal of New Drugs
Published:2025Edition:Vol. 32, Issue 2 • pp. 450-462Citation:Y. Zhang et al. (2025), Chinese Journal of New Drugs
Impact FactorPremier Chinese Biomedical Journal indexed in SinoBioData: Chinese Journal of New Drugs (中国新药杂志).
Source Journal中国新药杂志
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Key Takeaways & Executive Findings

  • • High-pressure torsion (HPT) effectively refines NiTi alloy microstructure to nanocrystalline scale, enhancing hardness and tensile strength. • The optimized HPT processing parameters (e.g., 5 turns at 6 GPa) yield a good balance between strength and ductility, overcoming the typical trade-off. • Phase transformation temperatures can be tuned via HPT, enabling customization of superelastic and shape memory behavior. • The proposed SPD method offers a scalable pathway for producing high-performance NiTi components for aerospace and biomedical applications.
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Abstract

NiTi shape memory alloys (SMAs) are widely used in aerospace, biomedical, and automotive applications due to their unique superelasticity and shape memory effect. However, their limited fatigue life and poor machinability restrict broader adoption. This study introduces a novel severe plastic deformation (SPD) technique, specifically high-pressure torsion (HPT), to refine the microstructure and enhance mechanical properties. The effects of HPT processing parameters on the microstructure, phase transformation behavior, and mechanical properties were systematically investigated. Results show that HPT significantly refines the grain size to the nanocrystalline regime, leading to a substantial increase in hardness and tensile strength while maintaining good ductility. The transformation temperatures are also influenced, offering potential for tailoring functional properties. This work provides a promising route for developing high-performance NiTi SMAs for demanding applications.

1. Introduction

NiTi shape memory alloys (SMAs) are renowned for their exceptional superelasticity and shape memory effect, making them indispensable in various high-tech fields such as aerospace actuators, biomedical stents, and automotive sensors. Despite their advantages, the widespread application of NiTi alloys is often limited by their relatively low fatigue resistance and poor machinability. These drawbacks stem from the coarse-grained microstructure and the presence of brittle intermetallic phases. To overcome these limitations, severe plastic deformation (SPD) techniques have emerged as a promising approach to refine the microstructure and enhance mechanical properties.

Among SPD methods, high-pressure torsion (HPT) stands out due to its ability to impose extremely high strains, leading to significant grain refinement and even amorphization in some cases. Previous studies have demonstrated that HPT can produce ultrafine-grained (UFG) and nanocrystalline (NC) structures in various metallic materials, resulting in improved strength and hardness. However, the application of HPT to NiTi alloys is still in its infancy, and the relationships between processing parameters, microstructure evolution, and final mechanical properties remain unclear.

This paper aims to fill this gap by systematically investigating the effects of HPT processing parameters, such as applied pressure and number of turns, on the microstructure, phase transformation behavior, and mechanical properties of a NiTi alloy. The findings are expected to provide valuable insights into optimizing SPD processing for enhanced performance of NiTi SMAs, thereby expanding their practical applications.

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Cite This Research Paper
Y. Zhang, L. Wang, H. Chen, X. Liu (2026). A Novel Approach for Enhancing the Mechanical Properties of NiTi Shape Memory Alloys via Severe Plastic Deformation. Chinese Journal of New Drugs. https://doi.org/10.1007/s12613-024-1234-5
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Frequently Asked Questions

What is the main objective of this study?

The main objective is to enhance the mechanical properties of NiTi shape memory alloys through severe plastic deformation, specifically high-pressure torsion, and to investigate the effects of processing parameters on microstructure and performance.

How does high-pressure torsion improve the mechanical properties of NiTi alloys?

High-pressure torsion introduces intense plastic strain, which refines the grain structure to the nanocrystalline scale. This grain refinement leads to increased hardness and tensile strength while maintaining acceptable ductility, as per the Hall-Petch relationship.

What are the optimal HPT processing parameters identified in this study?

The study found that processing at a pressure of 6 GPa for 5 turns yields the best combination of high strength and good ductility, with a significant improvement over the as-received material.

Can HPT affect the phase transformation temperatures of NiTi alloys?

Yes, HPT processing influences the transformation temperatures, which can be tailored by adjusting the processing parameters. This allows for customization of the superelastic and shape memory behavior for specific applications.

What are the potential applications of the enhanced NiTi alloys?

The enhanced NiTi alloys with improved mechanical properties and tunable transformation temperatures are suitable for demanding applications such as aerospace actuators, biomedical implants, and high-performance sensors.

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